Synthesis and properties of alkyl- and phenyltetrazolium picrates

Authors

  • П. Н. Гапоник Science Research Institute for Physicochemical Problems, Belorussian State University, Minsk 220080
  • C. B. Войтехович Science Research Institute for Physicochemical Problems, Belorussian State University, Minsk 220080
  • O. А. Ивашкевич Science Research Institute for Physicochemical Problems, Belorussian State University, Minsk 220080
  • А. C. Ляхов Science Research Institute for Physicochemical Problems, Belorussian State University, Minsk 220080
  • А. А. Говорова Science Research Institute for Physicochemical Problems, Belorussian State University, Minsk 220080

Abstract

A series of tetrazolium picrates has been synthesized by quaternization of C- and N-mono substituted tetrazoles using dimethylsulfate and the system t-BuOH/H2SO4 and subsequent precipitation of the cations formed with picric acid. Their thermal stability has been studied using differential scanning calorimetry and thermogravimetric analysis. An X-ray structural investigation has been carried out on 1,3-di-tert-butyl-5-methyltetrazolium picrate.

How to Cite
Gaponik, P. N.; Voitekhovich, S. V.; Ivashkevich, O. A.; Lyakhov, A. S.; Govorova, A. A. Chem. Heterocycl. Compd. 1998, 34, 579. [Khim. Geterotsikl. Soedin. 1998, 34, 657.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF02290942

Downloads

Published

1998-05-25

Issue

No. 5 (1998)

Section

Original Papers