N-3-oxoalkylamides and-thioamide in the synthesis of heterocyclic compounds. Part 1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions based on it

Authors

  • А. С. Фисюк Omsk State University, Omsk 644077
  • Л. В. Бердович Omsk State University, Omsk 644077
  • Д. В. Темников Omsk State University, Omsk 644077
  • Л. Н. Князькова Omsk State University, Omsk 644077

Abstract

The reaction of 3-isothiocyanatobutanal with ethanol in the presence of ethyl orthoformate produced 1,1-diethoxy-3-isothiocyanatobutane. The latter was used to devise methods of preparing 3-methylaminobutanal diethylacetal, N-(4-diethoxybutyl-2)thioamides, N-(4-oxybutyl-2)-thioamides, and 6-methyl-3-phenyl-5,6-dihydropyridine-2(1H)-thione.

How to Cite
Fisyuk, A. S.; Berdovich, L. V.; Temnikov, D. V.; Knyaz'kova, L. N.  Chem. Heterocycl. Compd. 1997, 33, 805. [Khim. Geterotsikl. Soedin. 1997, 921.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF02253030

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Published

1997-07-25

Issue

No. 7 (1997)

Section

Original Papers